柳明, 崔永亮, 王毅, 段又生, 芮昌辉, 王敏, 刘尚钟. N-苯基氨基邻苯二甲酰亚胺衍生物的合成及初步杀虫活性[J]. 农药学学报, 2009, 11(1): 51-54.
    引用本文: 柳明, 崔永亮, 王毅, 段又生, 芮昌辉, 王敏, 刘尚钟. N-苯基氨基邻苯二甲酰亚胺衍生物的合成及初步杀虫活性[J]. 农药学学报, 2009, 11(1): 51-54.
    shu
    LIU Ming, CUI Yong-liang, WANG Yi, DUAN You-sheng, RUI Chang-hui, WANG Min, LIU Shang-zhong. Synthesis and Preliminary Bioassay of N-Phenylaminophthalimide Derivatives[J]. Chinese Journal of Pesticide Science, 2009, 11(1): 51-54.
    Citation: LIU Ming, CUI Yong-liang, WANG Yi, DUAN You-sheng, RUI Chang-hui, WANG Min, LIU Shang-zhong. Synthesis and Preliminary Bioassay of N-Phenylaminophthalimide Derivatives[J]. Chinese Journal of Pesticide Science, 2009, 11(1): 51-54.
    shu

    N-苯基氨基邻苯二甲酰亚胺衍生物的合成及初步杀虫活性

    Synthesis and Preliminary Bioassay of N-Phenylaminophthalimide Derivatives

      摘要
    • 摘要: 为寻找新型环境友好型杀虫剂,用取代苯酐与取代苯肼在冰乙酸中缩合,合成了11个未见杀虫活性报道的N-苯基氨基邻苯二甲酰亚胺衍生物,其中7个是新化合物。所有化合物结构均通过核磁共振氢谱及液质联机(LC-MSD)确认,并利用X-ray单晶衍射确认了 A02 的晶体结构。初步的杀虫活性测试结果表明,大部分化合物对小菜蛾具有一定的杀虫活性,其中化合物 A06 在600 g/mL下96 h的致死率达到84％。

       

      Abstract: In order to discover novel environmental friendly insecticide,11 no insecticidal activity reported N-phenylaminophthalimide derivatives were synthesized through condensation reaction of substituted phthalic anhydride and substituted phenylhydrazine in glacial acetic acid,and 7 among them were new compounds.The structures of all compounds were confirmed with 1H NMR & LC-MSD,and the crystal structure of A02 was characterized by X-ray crystal diffraction method.The preliminary bioassay showed that some compounds had certain insecticidal activity against Plutella xylostella Linnaeus at 600 μg/mL,and the lethal rate of compound A06 was 84% after 96 hours.

       

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